Dispersibility Promotion of the Carbon Black Pigments and Optimization of the Process Via Response Surface Methodology (RSM)

Document Type : Research

Authors

1 Chemistry Department, Faculty of Basic Science, Azarbaijan Shahid Madani University, P. O. Code: 5375171379, Tabriz, Iran

2 Chemistry Department, Faculty of Basic Science, Azarbaijan Shahid Madani University, P. O. Code: 5375171379, Tabriz, Iran.

Abstract

One of the main problems of the paint and ink industry is the dispersion of carbon black in water-based media. Surface modification of the particles was used as an effective method to overcome the problem. Diazotized sulfanilic acid was used to modify the carbon black surface as the modifier. Due to the diversity of effective parameters and vast levels, the RSM method was used to find a suitable range of the parameters (temperature, modifier amount, ultrasonic time, and pH) at 5 levels. The properties of the modified pigment were analyzed by DLS, TGA/DTG, and FT-IR. Also, the accuracy of the modification was confirmed. Optimum conditions for modification were pH = 3.66, temperatures around 25 ℃, ultrasonic time of 30 minutes, and 6.25 mmol of the modifier. The optimally modified sample showed very high dispersion stability, so this sample has remained dispersed and stable for more than 8 months without any precipitation

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References

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Journal of Studies in Color World
Volume 12, Issue 2
October 2022
Pages 191-208

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History

  • Receive Date: 01 September 2022
  • Revise Date: 11 October 2022
  • Accept Date: 11 October 2022

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